Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 596380Generated: October 25, 2026

Potassium Iodide → HCID 68121467, compound

https://huagongshe.com/reaction/596380

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium IodideHCID 4875—
Reactant2-Buten-1-amineHCID 30447—
Reactant8-nitro-1-(chloromethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepineHCID 23337467—
SolventTetrahydrofuranHCID 8028—
ProductHCID 68121467HCID 68121467—

Reaction Steps

In the manner given in Preparation 39, 8-nitro-1-(chloromethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a]-[1,4]benzodiazepine, potassium iodide, and methylallylamine in tetrahydrofuran are reacted to give 8-nitro-1-[(allylmethylamino)methyl]-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine. Preparation 42 8-Bromo-1-[(allylethylamino)methyl]-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04010177
Source datasetuspto-grants-1977_03
ORD IDord-260832b30fe1435cb233aebd5e34029b
Source noteuspto-grants-1977_03