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HRID596380

反应详情

EQUATION

反应方程式

HRID 596380 的结构方程式

REACTANTS

反应物

3
结构：[I-].[K+]
HCID4875

Potassium iodide

IK

结构：CC=CCN
HCID30447

But-2-en-1-amine

C4H9N

结构：O=[N+]([O-])c1ccc2c(c1)C(c1ccccc1Cl)=NCc1nnc(CCl)n1-2
HCID23337467

未命名化合物

PRODUCTS

生成物

1
结构：C=CCCNCc1nnc2n1-c1ccc([N+](=O)[O-])cc1C(c1ccccc1Cl)=NC2
HCID68121467

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

In the manner given in Preparation 39, 8-nitro-1-(chloromethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a]-[1,4]benzodiazepine, potassium iodide, and methylallylamine in tetrahydrofuran are reacted to give 8-nitro-1-[(allylmethylamino)methyl]-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine. Preparation 42 8-Bromo-1-[(allylethylamino)methyl]-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine

WORKUP

后处理

  1. customare reacted