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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 596386Generated: October 31, 2026

Potassium Iodide → HCID 68120688, compound

https://huagongshe.com/reaction/596386

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium IodideHCID 4875—
Reactant2-Buten-1-amineHCID 30447—
ReactantHCID 21450803HCID 21450803—
SolventTetrahydrofuranHCID 8028—
ProductHCID 68120688HCID 68120688—

Reaction Steps

In the manner given in Preparation 39, 9-(trifluoromethyl)-1-(chloromethyl)-6-phenyl-4H-s-triazolo[4,3-a]-[1,4]benzodiazepine, potassium iodide and methylallylamine in tetrahydrofuran are reacted to give 9-(trifluoromethyl)-1-[(allylmethylamino)methyl]-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine. Preparation 48 8-Chloro-1-(pyrrolidinomethyl)-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04010177
Source datasetuspto-grants-1977_03
ORD IDord-713ca653b7a24064997c34ebe5b2d899
Source noteuspto-grants-1977_03