Sodium Bicarbonate → HCID 21449798, compound

Participants

Reaction Steps

The procedure of Example 4 is repeated but 13 parts of 1-benzyl-4-amino-6-chloropyridazinium perchlorate is used and 10 parts of sodium bicarbonate is used instead of triethylamine. 9.6 parts (67.3% of theory) of 1-benzyl-4-aminopyridazinium perchlorate is obtained from the filtrate from the reaction mixture; C11H12O4N3Cl, melting point 127° to 129° C after having been recrystallized from water.

Provenance & Evidence