HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21449773, compound → HCID 21449783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21449773 | HCID 21449773 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 21449783 | HCID 21449783 | 62.1% |
Reaction Steps
The procedure of Example 4 is adopted but without triethylamine and 15.6 parts of 1-cyclohexyl-4-amino-6-chloropyridazinium perchlorate is used. 8.6 parts (62.1% of theory) of 1-cyclohexyl-4-aminopyridazinium perchlorate is obtained; C10H16O4N3Cl, melting point 114° to 116° C after having been recrystallized from water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011220 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-625792202beb435796e4de03ec860e46 |
| Source note | uspto-grants-1977_03 |