HCID 21449773, compound → HCID 21449783, compound

HRID 596426Notes

Reaction equation

HRID 596426 reaction equation
[Cl:1]([O-:5])(=[O:4])(=[O:3])=[O:2].[CH:6]1([N+:12]2[C:17](Cl)=[CH:16][C:15]([NH2:19])=[CH:14][N:13]=2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1>C(N(CC)CC)C>[Cl:1]([O-:5])(=[O:4])(=[O:3])=[O:2].[CH:6]1([N+:12]2[CH:17]=[CH:16][C:15]([NH2:19])=[CH:14][N:13]=2)[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11]1

Participants

3

Reactant 1

HCID 21449773HCID 21449773, compound

Product 1

HCID 21449783HCID 21449783, compoundYield 62.1%

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The procedure of Example 4 is adopted but without triethylamine and 15.6 parts of 1-cyclohexyl-4-amino-6-chloropyridazinium perchlorate is used. 8.6 parts (62.1% of theory) of 1-cyclohexyl-4-aminopyridazinium perchlorate is obtained; C10H16O4N3Cl, melting point 114° to 116° C after having been recrystallized from water.

Sources & evidence

ORD record
ord-625792202beb435796e4de03ec860e46
Source dataset
uspto-grants-1977_03
Patent number
US04011220

Reaction notes

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