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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 596499Generated: October 25, 2026

Dimethyldithiocarbamic acid, dimethylamine → alpha-(1-Nitroethyl)benzyl dimethyldithiocarbamate

https://huagongshe.com/reaction/596499

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyldithiocarbamic acid, dimethylamineHCID 11728—
Reactant(2-Nitro-2-propenyl)benzeneHCID 575754—
SolventCarbon DisulfideHCID 6348—
Productalpha-(1-Nitroethyl)benzyl dimethyldithiocarbamateHCID 21324624—

Reaction Steps

As in Example 17, reaction of (2-nitro-2-propenyl)benzene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide, gave α-(1-nitroethyl)benzyl dimethyldithiocarbamate melting at 92° C.-94° C. when recrystallized without heating from acetone-ethanol solution.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04011230
Source datasetuspto-grants-1977_03
ORD IDord-42b83970ab794375977e587eb15f3827
Source noteuspto-grants-1977_03