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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 596506Generated: October 30, 2026

Dimethyldithiocarbamic acid, dimethylamine → p-Isopropyl-alpha-(nitromethyl)benzyl dimethyldithiocarbamate

https://huagongshe.com/reaction/596506

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyldithiocarbamic acid, dimethylamineHCID 11728—
Reactantp-Isopropyl-beta-nitrostyreneHCID 2737867—
SolventCarbon DisulfideHCID 6348—
Productp-Isopropyl-alpha-(nitromethyl)benzyl dimethyldithiocarbamateHCID 21324607—

Reaction Steps

As in Example 17, reaction of p-isopropyl-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave p-isopropyl-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 119° C.-120° C. after recrystallization without heating from acetone-methanol solution.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04011230
Source datasetuspto-grants-1977_03
ORD IDord-0f750e2804cc4f2cac0bf7ad3717a307
Source noteuspto-grants-1977_03