HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyldithiocarbamic acid, dimethylamine → p-Methoxy-alpha-(nitromethyl)benzyl dimethyldithiocarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| Reactant | 4-Methoxy-beta-nitrostyrene | HCID 229843 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | p-Methoxy-alpha-(nitromethyl)benzyl dimethyldithiocarbamate | HCID 21324614 | — |
Reaction Steps
As in Example 17, reaction of p-methoxy-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave p-methoxy-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 86° C.-89° C. when recrystallized without heating from acetone-methanol solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011230 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-ea8216732bb84738b54a214081e7a237 |
| Source note | uspto-grants-1977_03 |