HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21450339, compound → HCID 21450328, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21450339 | HCID 21450339 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21450328 | HCID 21450328 | — |
Reaction Steps
6-(1-methylpropyl)-3-hydroxy-2-nitropyridine (23 g.) in 450 ml. of methanol is hydrogenated over 1 gm. of 5% palladium on carbon catalyst for 3 hours. The catalyst is removed on a filter and the filtrate is concentrated to dryness to give 2-amino-3-hydroxy-6-(1-methylpropyl)pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011326 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-34e1a4d30b794b70b3f954b91d990fde |
| Source note | uspto-grants-1977_03 |