Sodium hydride → 3-Methoxybenzaldehyde

HRID 596614노트

반응식

HRID 596614 반응식
[H-].[Na+].[I-].C[S+](C)C.[CH3:8][O:9][C:10]1[CH:11]=[C:12]([CH:16]=[CH:17][CH:18]=1)[CH:13]1[O:15]C1>>[CH3:8][O:9][C:10]1[CH:11]=[C:12]([CH:16]=[CH:17][CH:18]=1)[CH:13]=[O:15]

참가 물질

4

반응물 3

HCID 24758Sodium hydrideHCID 75127Trimethylsulfonium iodideHCID 979032-(3-Methoxyphenyl)oxirane

생성물 1

HCID 115693-Methoxybenzaldehyde

실험 절차

Following the procedure of Example 7 and employing 2.42 g. of sodium hydride, 9.46 g. of trimethylsulfonium iodide and 6.33 g. (0.046 mol) of m-methoxybenzaldehyde there is obtained m-methoxystyrene oxide.

출처 및 근거

ORD 기록
ord-9117baebc4c948938188a6ee1e1ed5a4
출처 데이터셋
uspto-grants-1977_03
특허 번호
US04011319

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