HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 3927375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | ST51021144 | HCID 243437 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 3927375 | HCID 3927375 | — |
Reaction Steps
A solution of 11.91 gm. (0.05 mole) of ethyl 3-nitro-oxanilate in 500 ml. of methylene chloride is cooled to 5° in an ice bath. There is added slowly, 25 ml. of dimethylamine and the mixture stirred for two hours in an ice-bath. The ice-bath is removed and the mixture allowed to stand at room temperature overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04011337 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-72dc7ace2cc94b2cb92412f4561e3f5b |
| Source note | uspto-grants-1977_03 |