Hydrochloric Acid → HCID 21450284, compound

HRID 596698Notes

Reaction equation

HRID 596698 reaction equation
C([O:4][C:5]1[CH:6]=[C:7]([CH:16]=[CH:17][C:18]=1[N+:19]([O-:21])=[O:20])[C:8]([CH:10]([CH3:15])[CH2:11][C:12]([OH:14])=[O:13])=[O:9])(=O)C.Cl>[OH-].[Na+]>[OH:4][C:5]1[CH:6]=[C:7]([CH:16]=[CH:17][C:18]=1[N+:19]([O-:21])=[O:20])[C:8]([CH:10]([CH3:15])[CH2:11][C:12]([OH:14])=[O:13])=[O:9]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21450265HCID 21450265, compound

Product 1

HCID 21450284HCID 21450284, compound

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent

Procedure

3-(3-Acetoxy-4-nitrobenzoyl)butyric acid was dissolved in dilute sodium hydroxide solution, and the solution was warmed on a steam bath, cooled and acidified with hydrochloric acid to give 3-(3-hydroxy-4-nitrobenzoyl)butyric acid.

Workup

  1. temperaturethe solution was warmed on a steam bath
  2. temperaturecooled

Sources & evidence

ORD record
ord-1dcd9be34b76428a842ca67bbef6ddaf
Source dataset
uspto-grants-1977_03
Patent number
US04011321

Reaction notes

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