HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyanopyridine → 3-Cyano-1-(2-oxo-2-phenylethyl)pyridin-1-ium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyanopyridine | HCID 79 | — |
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | 4-Cyanopyridine | HCID 7506 | — |
| Reactant | p-Chlorophenacyl bromide | HCID 68303 | — |
| Product | 3-Cyano-1-(2-oxo-2-phenylethyl)pyridin-1-ium bromide | HCID 2841386 | — |
Reaction Steps
Employing the procedure of Example II but replacing 4-cyanopyridine with a substantially equimolecular amount of 3-cyanopyridine and replacing 4-chlorophenacyl bromide with a substantially equimolecular amount of phenacyl bromide there is obtained N-(phenacyl) 3-cyanopyridinium bromide, a white solid soluble in water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029153 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-269e734c4f5a46459d6cafd6982e0127 |
| Source note | uspto-grants-1977_03 |