HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54246754, compound → HCID 7128961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54246754 | HCID 54246754 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 7128961 | HCID 7128961 | — |
Reaction Steps
35.0 Parts of benzyloxycarbonyl-D-alanine n-propylamide is dissolved in ethanol. Then, palladium black catalyst is added and the mixture is shaken at about 60 psi at room temperature for several hours or until one molecular equivalent of hydrogen has been absorbed. The catalyst is removed by filtration, and the resulting solution is decolorized with charcoal. Removal of the solvents under reduced pressure affords, as an oil, D-alanine n-propylamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04012367 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-ef8f15da04a048359d7e23197ea54959 |
| Source note | uspto-grants-1977_03 |