HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethinyl-2-(p-methoxybenzyl)-1,3,3-trimethyl-4-piperidinol → 4-Ethyl-2-(p-methoxybenzyl)-1,3,3-trimethyl-4-piperidinol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethinyl-2-(p-methoxybenzyl)-1,3,3-trimethyl-4-piperidinol | HCID 21448618 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Ethyl-2-(p-methoxybenzyl)-1,3,3-trimethyl-4-piperidinol | HCID 16726140 | — |
Reaction Steps
A solution of 56 g of 4-ethinyl-2-(p-methoxybenzyl)-1,3,3-trimethyl-4-piperidinol in 350 ml of methanol is subjected to hydrogenation at atmospheric pressure and room temperature, the catalyst being 5% palladium on charcoal (5 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04012392 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-a8869df48025470881be001b8a49e896 |
| Source note | uspto-grants-1977_03 |