HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 12366432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(Acetyloxy)-5-ethyl-4-methylbenzoic acid | HCID 12366423 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12366432 | HCID 12366432 | — |
Reaction Steps
A mixture of 2-acetoxy-5-ethyl-4-methylbenzoic acid (11.10 g) and thionyl chloride (20 ml) in dry benzene (100 ml) was heated under reflux for 6 hours, cooled and solvents removed in vacuo. The crude 2-acetoxy-5-ethyl-4-methylbenzoyl chloride was obtained as a liquid which was used as rapidly as possible in the next stage of the synthesis without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04012407 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-d2a4892efc7a4cf9a07371eed6c9562e |
| Source note | uspto-grants-1977_03 |