HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 21449481, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 12395586 | HCID 12395586 | — |
| Reactant | Sodium bis(2-methoxyethoxy)aluminiumhydride | HCID 21584525 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 21449481 | HCID 21449481 | — |
Reaction Steps
2-Methyl-2-isopropyl-6,7-dichloro-1,5-indan-diol is prepared following substantially the same procedure described in Example 4, Step E, using the following substances: 2-methyl-2-isopropyl-5-hydroxy-6,7-dichloro-1-indanone (8.2 g., .03 mole); sodium bis-(2-methoxyethoxy)aluminum hydride (70% in benzene [10 ml.]; and tetrahydrofuran (100 ml.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04012524 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-f555896eb91a4ddda5470c8fe4fec363 |
| Source note | uspto-grants-1977_03 |