HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Benzyl-2-methyl-5-hydroxy-6,7-dichloro-1-indanone → 2-Benzyl-2-methyl-6,7-dichloro-1,5-indandiol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Benzyl-2-methyl-5-hydroxy-6,7-dichloro-1-indanone | HCID 12395591 | — |
| Reactant | Sodium bis(2-methoxyethoxy)aluminiumhydride | HCID 21584525 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Benzyl-2-methyl-6,7-dichloro-1,5-indandiol | HCID 21449477 | — |
Reaction Steps
2-Benzyl-2-methyl-6,7-dichloro-1,5-indandiol is prepared following substantially the same procedure described in Example 4, Step E, using the following substances: 2-benzyl-2-methyl-5-hydroxy-6,7-dichloro-1-indanone (4.8 g., 0.015 mole); sodium bis-(2-methoxyethoxy)-aluminum hydride (70% in benzene [5 ml.]); and tetrahydrofuran (50 ml.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04012524 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-a0c2eb9c40704229be72267ec89af33c |
| Source note | uspto-grants-1977_03 |