HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12395589, compound → HCID 21449490, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12395589 | HCID 12395589 | — |
| Reactant | Sodium bis(2-methoxyethoxy)aluminiumhydride | HCID 21584525 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21449490 | HCID 21449490 | — |
Reaction Steps
2-Cyclopentyl-2,6-dimethyl-7-chloroindan-1,5-diol is prepared following substantially the same procedure described in Example 4, Step E, using the following substances: 2-cyclopentyl-2,6-dimethyl-5-hydroxy-7-chloro-1-indanone (8.37 g., 0.03 mole); sodium bis-(2-methoxyethoxy)-aluminum hydride (70% in [10 ml.]); and tetrahydrofuran (100 ml.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04012524 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-ab4d358bfcd9412f8e279b04a1e3a602 |
| Source note | uspto-grants-1977_03 |