Ammonia → HCID 70638421, compound

Participants

Reaction Steps

Ammonia under pressure is added to a solution of 4 parts of 2,3-diphenylallyl chloride in 44 parts of benzene at 70° for 24 hours. After that time, the solid is separated by filtration and the benzene solution is reduced to an oil under reduced pressure. The oil is dissolved in isopropanolic hydrochloric acid and then diluted with ethyl ether to precipitate a solid. The solid is collected by filtration and dried to yield pure 2,3-diphenylallylamine hydrochloride, displaying nuclear magnetic resonance maxima at about 240, 241, 413, 426 and 442 Hertz and represented by the following structural formula ##STR5##

Provenance & Evidence