HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 597184Generated: November 1, 2026
Methyl Acrylate → HCID 86734571, compound
https://huagongshe.com/reaction/597184
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | 1,4-Bis(trimethylsilyl)-1,4-dihydropyridine | HCID 13287114 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86734571 | HCID 86734571 | — |
Reaction Steps
Following the procedure of Example 1, 8.6 g (0.1 mol) of acrylic acid methyl ester are brought to reaction with 22.6 g (0.1 mol) of 1,4-bis-(trimethylsilyl)-1,4-dihydropyridine. Upon addition of 20 ml of tetrahydrofuran the mixture is stirred at 50°C for 70 hours. The distillation in high vacuum yields 21.1 g (68%) of 1,4-bis-(trimethylsilyl-2-(1-carbomethoxyethyl)-1,2-dihydropyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04013661 |
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| Source dataset | uspto-grants-1977_03 |
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| ORD ID | ord-5011cdfa9a6b43c6a093c1ad8f42830e |
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| Source note | uspto-grants-1977_03 |
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