HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 21446960, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 20381773 | HCID 20381773 | — |
| Product | HCID 21446960 | HCID 21446960 | — |
Reaction Steps
In the same way as described in example 1, 3-chloro-7-methyl-7H-indolo[3,2-b][1,5]benzoxazepine-6(5H)-one, phosphorous pentachloride and diethylamine were reacted and the solid product recrystallized from methanol for analysis, mp. 127°-8°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04013660 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-fd34b968f0c74bebb4319e4676ebe490 |
| Source note | uspto-grants-1977_03 |