Diethylamine → HCID 21446960, compound

HRID 597189Notes

Reaction equation

HRID 597189 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]2[NH:8][C:9]3[C:15](=O)[N:14]([CH3:17])[C:13]4[CH:18]=[CH:19][CH:20]=[CH:21][C:12]=4[O:11][C:10]=3[C:5]2=[CH:4][CH:3]=1.P(Cl)(Cl)(Cl)(Cl)Cl.[CH2:28]([NH:30][CH2:31][CH3:32])[CH3:29]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[C:6](=[N:8][C:9]3[C:10]=2[O:11][C:12]2[CH:21]=[CH:20][CH:19]=[CH:18][C:13]=2[N:14]([CH3:17])[C:15]=3[N:30]([CH2:31][CH3:32])[CH2:28][CH3:29])[CH:7]=1

Participants

4

Reactant 3

HCID 8021DiethylamineHCID 24819Phosphorus pentachlorideHCID 20381773HCID 20381773, compound

Product 1

HCID 21446960HCID 21446960, compound

Procedure

In the same way as described in example 1, 3-chloro-7-methyl-7H-indolo[3,2-b][1,5]benzoxazepine-6(5H)-one, phosphorous pentachloride and diethylamine were reacted and the solid product recrystallized from methanol for analysis, mp. 127°-8°.

Workup

  1. customwere reacted
  2. customthe solid product recrystallized from methanol for analysis, mp. 127°-8°

Sources & evidence

ORD record
ord-fd34b968f0c74bebb4319e4676ebe490
Source dataset
uspto-grants-1977_03
Patent number
US04013660

Reaction notes

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