N,N-Dimethyl-1,3-propanediamine → HCID 178483520, compound

HRID 597190Notes

Reaction equation

HRID 597190 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]2[NH:8][C:9]3[C:15](=O)[N:14]([CH3:17])[C:13]4[CH:18]=[CH:19][CH:20]=[CH:21][C:12]=4[O:11][C:10]=3[C:5]2=[CH:4][CH:3]=1.P(Cl)(Cl)(Cl)(Cl)Cl.[CH3:28][N:29]([CH3:34])[CH2:30][CH2:31][CH2:32][NH2:33]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[C:6](=[N:8][C:9]3[C:10]=2[O:11][C:12]2[CH:21]=[CH:20][CH:19]=[CH:18][C:13]=2[N:14]([CH3:17])[C:15]=3[NH:33][CH2:32][CH2:31][CH2:30][N:29]([CH3:34])[CH3:28])[CH:7]=1

Participants

4

Reactant 3

HCID 7993N,N-Dimethyl-1,3-propanediamineHCID 24819Phosphorus pentachlorideHCID 20381773HCID 20381773, compound

Product 1

HCID 178483520HCID 178483520, compound

Procedure

In the same way as described in example 1, 3-chloro-7-methyl-7H-indolo[3,2-b][1,5]benzoxazepine-6(5H)-one, phosphorous pentachloride and 3-dimethylaminopropylamine were reacted and the crude product recrystallized from acetonitrile for analysis, mp. 156°-7°.

Workup

  1. customwere reacted
  2. customthe crude product recrystallized from acetonitrile for analysis, mp. 156°-7°

Sources & evidence

ORD record
ord-9b8710b774074075bdee13488587bcbe
Source dataset
uspto-grants-1977_03
Patent number
US04013660

Reaction notes

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