HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethyl-1,3-propanediamine → HCID 178483520, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 20381773 | HCID 20381773 | — |
| Product | HCID 178483520 | HCID 178483520 | — |
Reaction Steps
In the same way as described in example 1, 3-chloro-7-methyl-7H-indolo[3,2-b][1,5]benzoxazepine-6(5H)-one, phosphorous pentachloride and 3-dimethylaminopropylamine were reacted and the crude product recrystallized from acetonitrile for analysis, mp. 156°-7°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04013660 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-9b8710b774074075bdee13488587bcbe |
| Source note | uspto-grants-1977_03 |