HRID597220

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID69110

Benzoyl chloride, 2-chloro-

C7H4Cl2O

HCID12210597

未命名化合物

PRODUCTS

生成物

HCID22749031

未命名化合物

收率 97%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

1-Aminopyridinium chloride (104 parts) and -chlorobenzoyl chloride (150 parts) were heated in xylene (750 parts) at 140° C for 4 hours. The solid product was filtered off and recrystallised from n-butanol to give 1-(p-chlorobenzamido)pyridinium chloride (209 parts, 97% yeild), melting point 241° C.

WORKUP

后处理

filtrationThe solid product was filtered off
customrecrystallised from n-butanol