HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → [(2,2,2-Trifluoroethyl)sulfanyl]acetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-[(2,2,2-Trifluoroethyl)sulfanyl]acetic acid | HCID 16790808 | — |
| Product | [(2,2,2-Trifluoroethyl)sulfanyl]acetyl chloride | HCID 21816785 | — |
Reaction Steps
Thionyl chloride (21.9 g, 184 mmol) and trifluoroethylmercaptoacetic acid (15.9 g, 91 mmol) were stirred together overnight. The excess reagent was removed in vacuo and the product was distilled; bp 62°-68°/20 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04013765 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-4731bbfdd28c484b92a2595326397578 |
| Source note | uspto-grants-1977_03 |