HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanethiol → HCID 21445072, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanethiol | HCID 15290 | — |
| Reactant | HCID 21445066 | HCID 21445066 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 21445072 | HCID 21445072 | 74.8% |
Reaction Steps
12.1 g (50 m-moles) of 2-ethyl-4-chloro-5-nitro-6-isopropylamino-pyrimidine (vide Ex. 9a) are reacted with 7.0 g (60 m-moles) of cyclohexylmercaptan and 6.1 g (60 m-moles) of triethylamine to yield 12.0 g of 2-ethyl-4-cyclohexylthio-5-nitro-6-isopropylamino-pyrimidine of m.p. 69°-71° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04014677 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-a6a4cfb8082341159d2eacdb27d4361f |
| Source note | uspto-grants-1977_03 |