HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 86734583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 86734584 | HCID 86734584 | — |
| Reactant | 1,3-benzoxazole-2-thiol | HCID 178418282 | — |
| Product | HCID 86734583 | HCID 86734583 | — |
Reaction Steps
10 parts of sodium salt of 2-mercaptobenzoxazole and 13.32 parts of N-(2-cyanoethyl)-N-(α-chloroacetoxyethyl)-aniline in 200 parts of xylene and 40 parts of dimethyl formamide is boiled under reflux for 24 hours. It is worked up in the manner described in Instruction-1 to furnish N-(2-cyanoethyl)-N-(benzoxazolyl-2-thioacetoxy ethyl) aniline having the formula ##STR17##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04014864 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-69c966c6df6f44beb8398db142eec96b |
| Source note | uspto-grants-1977_03 |