HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Azido-4-phenylcarbostyril → 5,7-Dihydro-6H-indolo[2,3-c]quinolin-6-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Azido-4-phenylcarbostyril | HCID 21445440 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 5,7-Dihydro-6H-indolo[2,3-c]quinolin-6-one | HCID 21445410 | — |
Reaction Steps
A suspension of 114 g. of 3-azido-4-phenylcarbostyril in 2 l. of toluene was heated to reflux until nitrogen evolution ceased (5 hours). On cooling, 7H-indolo[2,3-c]quinolin-6(5H)-one crystallized; 84.7 g. (84 percent), having a melting point of 314°-316° .
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04014883 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-5d91ec22b5fb4b4598e6fe69f48e7afd |
| Source note | uspto-grants-1977_03 |