HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21414243, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21414233 | HCID 21414233 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 21414243 | HCID 21414243 | — |
Reaction Steps
1,1a,6,10b-Tetrahydrodibenzo[a,e]cyclopropa[c]cyclohepten-6-one O-[2-(dimethylamino)ethyl]oxime prepared as in Example 1 was dissolved in ether and saturated with anhydrous hydrogen chloride. The precipitate was filtered and thoroughly washed with ether. The product was recrystallized from acetonitrile, and dried at 100° (0.1 mm), mp 169°-171° .
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04014936 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-eb4ff10fc5ed4ca1b18d5a8f0c561713 |
| Source note | uspto-grants-1977_03 |