HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N-((4-(((4-bromophenethyl)(piperidin-4-yl)amino)methyl)phenyl)sulfonyl)acetamide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 121410336 | HCID 121410336 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | N-((4-(((4-bromophenethyl)(piperidin-4-yl)amino)methyl)phenyl)sulfonyl)acetamide hydrochloride | HCID 121410314 | — |
Reaction Steps
tert-Butyl 4-((4-(N-acetylsulfamoyl)benzyl)(4-bromophenethyl)amino)piperidine-1-carboxylate obtained in Step 1 was subjected to the deprotection reaction as described in Procedure 2 (4 N HCl in EtOAc). The crude product was carried on to the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440953B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-4c2f6e14737443418775cf70074460c6 |
| Source note | uspto-grants-2016_09 |