HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178475154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | N-((4-(((4-bromophenethyl)(piperidin-4-yl)amino)methyl)phenyl)sulfonyl)acetamide hydrochloride | HCID 121410314 | — |
| Reactant | N-cyanopiperazine-1-carbimidothioate | HCID 131737066 | — |
| Product | HCID 178475154 | HCID 178475154 | — |
Reaction Steps
N-((4-(((4-Bromophenethyl)(piperidin-4-yl)amino)methyl)phenyl)sulfonyl)acetamide hydrochloride obtained in Step 2 was reacted with K2CO3 and S,S′-dimethyl-N-cyano-dithioiminocarbonate, followed by the cyclization of the intermediate (N-cyanopiperazine-1-carbimidothioate) with hydrazine monohydrate in a manner described in Procedure 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440953B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-d1c81bf415924904b5e3a8cac6d77f51 |
| Source note | uspto-grants-2016_09 |