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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 598100Generated: October 31, 2026

Potassium Hydroxide → HCID 58938534, compound

https://huagongshe.com/reaction/598100

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium HydroxideHCID 14797—
ReactantHCID 58938583HCID 58938583—
SolventEthanolHCID 702—
ProductHCID 58938534HCID 5893853483.6%

Reaction Conditions

Temperature60 °C

Reaction Steps

Ethyl 1-(dipropylamino)-6-mesityl-4-oxo-4H-quinolizine-3-carboxylate (0.0145 g, 0.033 mmol) was dissolved in ethanol (0.3 mL). Potassium hydroxide (6M in ethanol, 94 μL, 0.57 mmol) was added. The solution was heated at 60° C. for 1 h. The solution was extracted using ethyl acetate, dried over magnesium sulfate and concentrated to give 0.010 g (83% yield) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07897607B2
Source datasetuspto-grants-2011_03
ORD IDord-4db8714ab5fd429e9647b5df2bba433f
Source noteuspto-grants-2011_03