HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexyl isocyanate → HCID 67268410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexyl isocyanate | HCID 75659 | — |
| Reactant | HCID 67268948 | HCID 67268948 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 67268410 | HCID 67268410 | — |
Reaction Steps
Analogously to Example 1, tert-butyl 7-methyl-2-oxo-2,3-dihydroimidazo[4,5-b]pyridine-1-carboxylate (300 mg, 1.2 mmol), 1-isocyanatohexane (183.8 mg, 1.44 mmol) and 4-dimethylaminopyridine (14.7 mg, 0.12 mmol) were reacted in toluene. Yield: 8 mg (2%), M+H+: 277.16.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897616B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-15b6fea5e0374100bf33be655bbcc309 |
| Source note | uspto-grants-2011_03 |