HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → N-Hexyl-7-methyl-2-oxo-1,2-dihydroimidazo[4,5-c]pyridine-3-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Hexyl isocyanate | HCID 75659 | — |
| Reactant | 3H-Imidazo[4,5-c]pyridin-2-ol | HCID 11686916 | — |
| Product | N-Hexyl-7-methyl-2-oxo-1,2-dihydroimidazo[4,5-c]pyridine-3-carboxamide | HCID 67268408 | — |
Reaction Steps
Analogously to Example 1, 2 g (14.8 mmol) of 1,3-dihydroimidazo[4,5-c]pyridin-2-one and 1-isocyanatohexane (2.26 g, 17.76 mmol) were reacted in toluene. Yield: 43 mg (1%), M+H+: 263.19.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897616B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-42ff90f4494d4f448037cbeda38cdd5a |
| Source note | uspto-grants-2011_03 |