HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzyl cyanide → HCID 73050958, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzyl cyanide | HCID 241582 | — |
| Reactant | 1-(4-chloro-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole | HCID 90032549 | — |
| Product | HCID 73050958 | HCID 73050958 | — |
Reaction Steps
The title compound, light green solid (111 mg, 82%), MS (ISP) m/z=406.2 [(M+H)+], mp 222° C., was prepared in accordance with the general method of example 1 from 1-(4-chloro-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole (intermediate H) (100 mg, 353 μmol) and commercially available 2-(4-chloro-phenyl)-acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440962B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-a072745296e4448e8daf6fc2855c6c8d |
| Source note | uspto-grants-2016_09 |