HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzeneacetonitrile, 4-fluoro- → HCID 73051256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzeneacetonitrile, 4-fluoro- | HCID 68016 | — |
| Reactant | 1-(2-chloro-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole | HCID 90032551 | — |
| Product | HCID 73051256 | HCID 73051256 | — |
Reaction Steps
The title compound, green solid (53 mg, 41%), MS (ISP) m/z=390.2 [(M+H)+], mp 161° C., was prepared in accordance with the general method of example 1 from 1-(2-chloro-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole (intermediate L) (100 mg, 353 μmol) and commercially available 2-(4-fluoro-phenyl)-acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440962B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-74d0ce3b928a4390bcc45a40b8c6d8d2 |
| Source note | uspto-grants-2016_09 |