関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 反応物 | Methyl 4-acetylbenzoate | HCID 137990 | — |
| 生成物 | Methyl 4-[3-(dimethylamino)prop-2-enoyl]benzoate | HCID 10561611 | — |
反応手順
A mixture of methyl 4-acetylbenzoate (5.00 g, 28.1 mmol) in DMF-DMA (38 mL, 284 mmol) was heated at 105° C. for 20 hours. The reaction was cooled, concentrated, and used crude in the next reaction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US09440964B2 |
|---|
| 出典データセット | uspto-grants-2016_09 |
|---|
| ORD ID | ord-8ca3e56aacc74e2aae48df2c703518c5 |
|---|
| 出典メモ | uspto-grants-2016_09 |
|---|
