HRID599355

反应详情

EQUATION

反应方程式

HRID 599355 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

0.04 g of 1-[(4-pyridin-3-yl-8-azabicyclo[3.2.1]oct-8-yl)carbonyl]-1,2,3,4-tetrahydroquinoline is dissolved in 1.15 ml of a 0.2N solution of hydrochloric acid in ether. After evaporation, the residue is taken up in ethyl acetate. The precipitate is filtered off and then dried under vacuum. 0.004 g of 1-[(4-pyridin-3-yl-8-azabicyclo[3.2.1]oct-8-yl)carbonyl]-1,2,3,4-tetrahydroquinoline hydrochloride is obtained.

WORKUP

后处理

  1. customAfter evaporation
  2. filtrationThe precipitate is filtered off
  3. customdried under vacuum