HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxygen → Acetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxygen | HCID 977 | — |
| Reactant | 1-Phenylethanol | HCID 7409 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Water | HCID 962 | — |
| Product | Acetophenone | HCID 7410 | 82% |
Reaction Steps
In an ambient pressure oxygen atmosphere, 121 μl of 1-phenyl ethanol and 173.7 mg of the platinum catalyst obtained in Example 1 were agitated for twenty-four hours at 60° C. in 10 ml of water. The reaction mixture was subsequently extracted using ethyl acetate, and the organic layer was dried using magnesium sulfate and filtered to obtain 98.9 mg (82% yield) of acetophenone. The reaction equation and the analytical results of the product are shown below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897817B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-9343fef9a294494c9c4edbca096df93a |
| Source note | uspto-grants-2011_03 |