HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxygen → Cyclooctanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxygen | HCID 977 | — |
| Reactant | Cyclooctanol | HCID 12766 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Water | HCID 962 | — |
| Product | Cyclooctanone | HCID 10403 | 93% |
Reaction Steps
In an ambient pressure oxygen atmosphere, 25 mg of cyclooctanol and 137 mg of the platinum catalyst obtained in Example 1 were agitated for sixty hours at 60° C. in 2 ml of water. The reaction mixture was subsequently extracted using ethyl acetate, and the organic layer was dried using magnesium sulfate, filtered and concentrated to obtain 22.8 mg (93% yield) of cyclooctanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897817B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-ec3f67895077445987c8528253357f5c |
| Source note | uspto-grants-2011_03 |