Palladium Chloride → HCID 22617121, compound

Participants

Reaction Steps

Palladium chloride (3.00 g; manufactured by Wako Pure Chemical Industry), 2.10 g of lithium chloride (manufactured by Wako Pure Chemical Industry) and 40 mL of methanol were charged in a flask made of glass where the inner air was substituted with highly pure argon and were stirred for 4 hours. Norbornadiene (2.1 g; manufactured by Aldrich) was added to the resulting homogeneous solution and the mixture was stirred for 12 hours. The resulting yellow solid was sucked to give 3.6 g of norbornadiene dichloropalladium.

Provenance & Evidence