Sodium Methoxide → HCID 86634829, compound

Participants

Reaction Steps

The above-prepared norbornadiene dichloropalladium (1.40 g) was added to 20 mL of methanol in a flask made of glass where inner air was substituted with highly pure argon and then the inner temperature was made −40° C. using a dry ice bath. Into this was dropped 1.5 mL of a 28% methanolic solution of sodium methoxide (manufactured by Wako Pure Chemical Industry). The mixture was made to react for 1 hour and returned to room temperature. The resulting yellow solid was sucked and washed with methanol to give 1.22 g of methoxynorbornene palladium chloride dimer.

Provenance & Evidence