cis,cis-1,5-Cyclooctadiene → HCID 2733356, compound

Participants

Reaction Steps

Palladium chloride (3.0 g; manufactured by Wako Pure Chemical Industry), 2.1 g of lithium chloride (manufactured by Wako Pure Chemical Industry) and 40 mL of methanol were charged in a flask made of glass where inner air was substituted with highly pure argon and were stirred for 4 hours. 1,5-Cyclooctadiene (2.31 g; manufactured by Wako Pure Chemical Industry) was added to the resulting homogeneous solution and the mixture was stirred for 12 hours. The resulting yellow solid was sucked to give 4.82 g of 1,5-cyclooctadiene dichloropalladium.

Provenance & Evidence