HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → HCID 67273095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | (S)-(+)-1-(2-Pyrrolidinylmethyl)pyrrolidine | HCID 853152 | — |
| Reactant | 6-Bromo-2-tetralone | HCID 2733553 | — |
| Reactant | HCID 63625845 | HCID 63625845 | — |
| Product | HCID 67273095 | HCID 67273095 | — |
Reaction Steps
(6-Butylamino-5,6,7,8-tetrahydro-naphthalen-2-yl)-(2-pyrrolidin-1-ylmethyl-pyrrolidin-1-yl)-methanone is prepared from (6-bromo-1,2,3,4-tetrahydro-naphthalen-2-yl)-butyl-amine and (S)-(+)-1-(2-pyrrolidinylmethyl)-pyrrolidine in a manner substantially analogous to Procedure A. (See herein Example 1). Starting material, (6-bromo-1,2,3,4-tetrahydro-naphthalen-2-yl)-butyl-amine, was prepared from 6-bromo-2-tetralone and n-butylamine in a manner substantially analogous to Preparation 1. Mass spectrum (APCI) 384 (M++1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902191B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-e920fe347c4f450892e43e6bb2fced5e |
| Source note | uspto-grants-2011_03 |