HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 67273847, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Sodium Dithionite | HCID 24489 | — |
| Reactant | HCID 67273481 | HCID 67273481 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67273847 | HCID 67273847 | — |
Reaction Steps
0.42 g of 2-benzoyl-6-nitroimidazo[1,2-a]pyridine in 20 mL of boiling ethanol is treated with 10 mL of 0.5 N sodium hydroxide solution and 2.77 g of sodium dithionite. After 10 minutes at 80° C., the reaction medium is cooled, filtered and concentrated to dryness to give the crude (6-aminoimidazo[1,2-a]pyridin-2-yl)(phenyl)methanone, which is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902219B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-598a927f9d684d0b937799d8892e411e |
| Source note | uspto-grants-2011_03 |