HRID601094

反应详情

EQUATION

反应方程式

HRID 601094 的结构方程式

PROCEDURE

实验过程

Using an analogous procedure to the synthesis of 2,4-bis(tert-butyl)-6-[[(2,6-dibromophenyl)amino]methyl]phenol described above, NaBH4 (0.8 g) was added to a solution of 2,4-bis(tert-butyl)-6-[[(2,6-dichlorophenyl)imino]methyl]phenol (0.91 g, 2.41 mmol). The product was purified from hot hexane and isolated as colourless crystals. Yield 0.61 g, 67%.

WORKUP

后处理

  1. customThe product was purified from hot hexane
  2. customisolated as colourless crystals