HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-[(2-ethylbutyl)amino]nicotinate → 1-Benzyl-7-methyl-2H-pyrido[2,3-d][1,3]oxazine-2,4(1H)-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-[(2-ethylbutyl)amino]nicotinate | HCID 67064133 | — |
| Reactant | HCID 86592109 | HCID 86592109 | — |
| Product | 1-Benzyl-7-methyl-2H-pyrido[2,3-d][1,3]oxazine-2,4(1H)-dione | HCID 49758043 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 3B substituting the product of Example 62A for the product of Example 3A (0.150 g, 50%). 1H NMR (300 MHz, CDCl3) δ 2.66 (s, 3H), 5.47 (s, 2H), 7.10 (d, J=8.09 Hz, 1H), 7.31 (m, 3H), 7.55 (dd, J=7.54, 1.65 Hz, 2H), 8.26 (d, J=8.09 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902203B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-4b358f14345a4690a9f0ace4a1e2b720 |
| Source note | uspto-grants-2011_03 |